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Edge-carboxylated graphene nanosheets via ball milling:

Jeon, In-Yup ; Shin, Yeon-Ran ; Sohn, Gyung-Joo...
Proceedings of the National Academy of Sciences.  109 (2012)  15 - p. 5588-5593 , 2012
Link: https://doi.org/10.1073/pnas.1116897109